| 高文涛,符鑫博,李阳.化学通报,2016,79(7):630-639,644. |
| (E)-6-氯-2-芳乙烯基-3-喹啉甲酸衍生物的合成 |
| Syntheses of Novel (E)-6-chloro-2-arylvinylquinoline-3-formic Acid Derivatives |
| 投稿时间：2015-10-27 修订日期：2015-11-23 |
| DOI： |
| 中文关键词: 6-氯-2-氯甲基-3-喹啉甲酸乙酯，芳香醛，2-苯乙烯基喹啉，喹啉甲酸，衍生物 |
| 英文关键词:Ethyl 6-chloro-2-(chloromethyl)quinoline-3-carboxylate, Aromatic aldehydes, 2-Styrylquinoline, Quinoline-formic acid, Derivatives |
| 基金项目:国家自然科学基金项目（21476028） |
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| 中文摘要: |
| 以6-氯-2-氯甲基-3-喹啉甲酸乙酯(1)与芳香醛类化合物3a-f′为起始化合物，通过简便有效的“一锅法”反应，合成了(E)-6-氯-2-芳乙烯基-3-喹啉甲酸衍生物4a-f′。所合成的32个化合物4a-f′均未见文献报道，其结构经红外光谱、核磁共振氢谱、核磁共振碳谱和高分辨质谱得以确认。 |
| 英文摘要: |
| In this paper, (E)-6-chloro-2-arylvinylquinoline-3-formic acid derivatives 4a-f′ was synthesized through a simple and efficient one-pot reaction from ethyl 6-chloro-2-(chloromethyl)quinoline-3-carboxylate (1) and various aromatic aldehydes 3a-f′. The newly synthesized 32 compounds are firstly reported, and their structures had been characterized by IR, 1H NMR, 13C NMR and HR-MS. |
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